개질한 지르코니아를 함유한 열경화성 액정 에폭시의 열분해 거동

Thermal Decomposition Behavior of LCT Composites with Modified Zirconia Filler

초록

In this study, liquid crystalline thermosetting epoxy resin (LCTER) was synthesized with 4,4'-diglycidyloxy-α-methylstilbene and sulfanilamide as a basic resin and curing agents, respectively. Following the synthesis, the LCTER composite was fabricated using modified zirconia as a filler. To investigate the thermal behavior of the LCTER composites, a thermogravimetric analysis of the LCTER composites was recorded on temperature difference, with a filler content of 0.5–5 wt% of modified zirconia. The activation energy for the thermal decomposition was calculated using the Kissinger and Flynn–Wall methods. It was found that the activation energies of LCTER composites were proportional to the amount of modified zirconia used in the composites.

키워드

liquid crystalline thermosetting epoxy; modified zirconia; activation energy for thermal decomposition; Kissinger method; Flynn-wall method
제목
개질한 지르코니아를 함유한 열경화성 액정 에폭시의 열분해 거동
제목 (타언어)
Thermal Decomposition Behavior of LCT Composites with Modified Zirconia Filler
저자
문희정; 조승현
발행일
2016-08
저널명
한국섬유공학회지
권
53
호
4
페이지
293 ~ 298